Comparison of Heating Methods and Heating Characteristics of Dry Nitrogen Blowing Apparatus and Water Bath Nitrogen Blowing Apparatus

Dry nitrogen blower heating method:

The dry nitrogen blowing instrument can quickly evaporate and separate the solvent in the sample by blowing nitrogen into the surface of the heated sample to achieve the purpose of oxygen-free concentration of the sample, and keep the sample more pure. Concentration using a nitrogen blower instead of a conventional rotary evaporator allows for the simultaneous concentration of dozens of samples, saving time and efficiency.

Dry nitrogen blowing instrument heating features:

1. The heater causes the sample to be rapidly heated to the evaporation temperature, while the gas is blown through the gas needle to the surface of the solution, causing rapid evaporation of the solution and concentration of the sample.

2. The position of the gas needle in the air chamber can be changed to suit different test tubes.

3. When concentrating toxic solvents, the entire system can be placed in a fume hood.

Water bath nitrogen blowing instrument heating method:

A water bath nitrogen blower concentrates the sample by blowing nitrogen into the surface of the heated sample. The method has the characteristics of convenient operation and easy control, and can quickly obtain the expected result.

Water bath nitrogen blowing instrument refueling features:

1. Water bath heating usually puts the test tube to be heated in a water-filled beaker. The heat source heats the water, and the water transfers the heat to the test tube. It can be regarded as an indirect heating process, which is different from the dry direct contact heat source heating. In addition, due to the heating process of the water bath, a thermometer can be inserted in the water of the beaker to observe the water temperature in real time, so that the temperature of the water can be well controlled, and the dry heating method is difficult to realize real-time temperature control.

2. During the heating process of the water bath, the test tube is immersed in the beaker water, and the parts are heated more uniformly; while the dry heating method is usually the bottom of the test tube is heated more than the upper part.

3. The heating of the water bath is slow and the temperature is slow, and the heating temperature does not exceed 100 °C. It is a kind of "gentle" heating method; the dry heating method has a rapid temperature drop and a rapid heating temperature, and the heating temperature can be as high as 180 °C, which can be considered as a kind. "Quick fire" heating, two heating methods are suitable for different material samples.

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